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Part 1 Experimental Organic Chemistry

Chapter 1 General Introduction// 3

1. Laboratory Rules// 3

2. Safety Rules and Regulations in Chemistry Laboratory // 3

3. Treatment of the Common Accidents in Laboratory// 5

4. Fire Prevention and Treatment // 5

5. First Aid Kit// 5

6. Preview, Record and Laboratory Report// 5

Chapter 2 Common laboratory Apparatus and Equipment // 7

1. General Glassware // 7

2. Common Standard-taper Glassware// 7

3. Common Glass Apparatus// 8

4. Common Equipment // 8

Chapter 3 Laboratory Experiments// 11

Experiment 1 Basic Laboratory Techniques (¢ñ) // 11

Experiment 2 Basic Laboratory Techniques (¢ò) // 14

Experiment 3 Extraction of Iodine// 16

Experiment 4 Determination of the Melting Point// 18

Experiment 5 Micro Determination of the Boiling Point// 19

Experiment 6 Refractive Index Determination of Liquid Organic Compound // 21

Experiment 7 Operation of Organic Molecular Models// 23

Experiment 8 Paper Electrophoresis of Amino Acid// 25

Experiment 9 Column Chromatography// 27

Experiment 10 Thin-Layer Chromatography (TLC) // 29

Experiment 11 Paper Chromatography// 31

Experiment 12 Preparation of Aspirin // 34

Experiment 13 Preparation of Acetanilide // 36

Experiment 14 Extraction of Rutin and Recovery of Extraction Agent// 38

Experiment 15 Analysis of Unknown Sample of Organic Compounds (Designing Experiment)// 39

Part 2 Solutions Manual for Organic Chemistry

Chapter Introduction// 43

Chapter Saturated Hydrocarbons: Alkanes and Cycloalkanes // 45

Chapter Unsaturated Hydrocarbons: Alkenes, Alkynes and Aromatics// 48

Chapter Alcohols, Phenols, and Ethers// 51

Chapter Aldehydes and Ketones // 55

Chapter Carboxylic Acids and Acid Derivatives// 59

Chapter Amines // 64

Chapter Optical Isomerism// 66

Chapter Carbohydrate// 70

Chapter Lipids// 73

Chapter Proteins // 76

Chapter Nucleic Acids// 79

References // 80