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**²¿·Ö Óлú»¯Ñ§ÊµÑéµÄÒ»°ã֪ʶ Ò»¡¢ÊµÑéÊÒ¹æÔò ¶þ¡¢ÊµÑéÊҵݲȫ Èý¡¢Óлú»¯Ñ§ÊµÑé·ÏÎïµÄ·ÖÀàºÍ´¦Öà ËÄ¡¢ÊµÑéÊÒ³£ÓÃÒÇÆ÷É豸ºÍ¼¼Êõ Îå¡¢³£ÓÃÓлúÈܼÁ¼°´¿»¯ Áù¡¢ÄƵÄʹÓü°´¦Àí Æß¡¢ÊµÑéÇ°×¼±¸¼°ÊµÑé¼Ç¼ºÍ±¨¸æ Part ¢ñ General Knowledge of Organic Chemistry Experiments ¢ñ£®General Laboratory Rules ¢ò£®Laboratory Safety ¢ó£®Disposal of Laboratory Waste ¢ô£®Common Apparatus and Techniques ¢õ£®Common Organic Solvents ¢ö£®Use and Disposal of Sodium ¢÷£®Advance Preparation and Lab Record and Report µÚ¶þ²¿·Ö »ù±¾²Ù×÷ʵÑé Part ¢ò Basic Techniques ʵÑéÒ» ÈÛµã²â¶¨ Experiment Melting Point Determination ʵÑé¶þ ·Ðµã²â¶¨ Experiment 2 Boiling Point Determination ʵÑéÈý Öؽᾧ Experiment 3 RecrystazafiOn ʵÑéËÄ ³£Ñ¹ÕôÁó Experiment 4 Simple Distillation ʵÑéÎå ·ÖÁó Experiment 5 Fractional Distillation ʵÑéÁù Ë®ÕôÆøÕôÁó Experiment 6 Steam Distillation ʵÑéÆß ¼õѹÕôÁó Experiment 7 Vacuum Distillation ʵÑé°Ë ·ÖҺ©¶·ÝÍÈ¡ Experiment 8 Extractions Using Separatory Funnels ʵÑé¾Å ±¡²ãÉ«Æ׺ÍÖùÉ«Æ× Experiment 9 Thin-Layer and Column Chromatography µÚÈý²¿·Ö »ù´¡ÐÔÓлúºÏ³ÉʵÑé Part ¢ó Basic Organic Synthetic Experiments ʵÑéÊ® äåÒÒÍéÖƱ¸ Experiment 10 Preparation of Ethyl Bromide ʵÑéʮһ »·¼ºÏ©µÄÖƱ¸ Experiment 11 Preparation of Cyclohexene ʵÑéÊ®¶þ ÒÒõ£±½°·ÖƱ¸ Experiment 12 Preparation of Acetanilide ʵÑéÊ®Èý ÒÒõ£ÒÒËáÒÒõ¥µÄÖƱ¸ Experimental 13 Preparation of Ethyl Acetoacetate ʵÑéÊ®ËÄ äå±½ÖƱ¸ Experiment 14 Preparation of Bromobenzene ʵÑéÊ®Îå ±½¼×ËáÒÒõ¥µÄÖƱ¸ Experiment 15 Preparation of Ethyl Benzoate ʵÑéÊ®Áù Èý±½¼×´¼µÄÖƱ¸ Experiment 16 Preparation of Triphenylmethanol ʵÑéÊ®Æß 2-Ïõ»ùÀ×Ëö·ÓµÄÖƱ¸ Experiment 17 Preparation of 2£®NitroresOrcinOl ʵÑéÊ®°Ë ·¼ÏãÈ©µÄ¿µÄá²éÂÞ·´Ó¦ Experiment 18 Cannizzaro Reaction of Aryl Aldehydes ʵÑéÊ®¾Å à­ßøµÄÖƱ¸ Experiment 19 Preparation of Quinoline ʵÑé¶þÊ®¶þ ±½ôÇÒÒËáµÄÖƱ¸ Experiment 20 Preparation of Benzilic Acid ʵÑé¶þʮһ »·¼ºÍªë¿µÄ±´¿ËÂüÖØÅÅ Experiment 21 Beckmann Rearrangement of Cyclohexanone Oxime ʵÑé¶þÊ®¶þ 7£¬7Ò»¶þÂÈË«»·[4£¬1£¬0]¸ýÍéµÄÖƱ¸¡ª¡ªÏàתÒÆ·¨ Experiment 22 Preparation of 7£¬7Ò»DlchIorobicycIo[4£®1£®0]heptane ʵÑé¶þÊ®Èý ¶þ±½¼×ͪµÄÖƱ¸ Experiment 23 Preparation of BenzODhenOne ʵÑé¶þÊ®ËÄ ÕÁÄԵĻ¹Ô­·´Ó¦ Experiment 24 The Reduction of Camphor µÚËIJ¿·Ö ×ÛºÏÐÔÓлúºÏ³ÉʵÑé Part ¢ô Comprehensive Organic Synthetic Experiments ʵÑé¶þÊ®Îå ÑÇÜлùÒÒõ£±½µÄÖƱ¸¼°ÆäÓëäåµÄ·´Ó¦ Experiment 25 Preparation of BenzalacetODhenOne and Its Reaction With Bromine ʵÑé¶þÊ®Áù ½µÑªÖ¬Ò©¼ª·ÇÂÞÆëÖмäÌå3Ò»(2£¬5Ò»¶þ¼×»ù±½Ñõ»ù)Ò»1Ò»ÂȱûÍéµÄÖƱ¸¼°·´Ó¦¹ý³Ì¸ú×Ù Experiment 26 Synthesis of 3Ò»(2£¬5-Xylyloxyl)propyl Chloride and Monitoration of Reaction Process ʵÑé¶þÊ®Æß 1Ò»±½»ùÒ»2Ò»¼×»ùÒ»2Ò»Ïõ»ù±û´¼µÄÖƱ¸¼°·´Ó¦¹ý³Ì¸ú×Ù Experiment 27 Preparation of 1Ò»Pheny1Ò»2Ò»methyl-2Ò»nitropropanol and Monitoration of Reaction Process µÚÎ岿·Ö Éè¼ÆÐÔÓлúºÏ³ÉʵÑé Part V Designing Organic Synthetic Experiment ʵÑé¶þÊ®°Ë Èâ¹ðËáµÄÖƱ¸ Experiment 28 Preparation of Cinnamic Acid ¸½Â¼