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**Õ  Ò»°ãÐÔʵÑéÖ¸µ¼chapter 1  general instructions     **½Ú  ʵÑéÊÒ°²È«ÊØÔò      section 1 laboratory safety    µÚ¶þ½Ú  ÌìƽʹÓùæ³Ì    section 2 protocol for using balance    µÚÈý½Ú  ÓÐЧÊý×ÖµÄÐÞÔ¼    section 3 rounding of significant figures    µÚËĽڠ Ò»°ãÐԹ涨һ    section 4 general noices    µÚÎå½Ú  ʵÑé¼Ç¼¼°±¨¸æ¸ñʽ    section 5 experiment record and report formatµÚ¶þÕ  Ò©ÎïµÄÐÔ×´¡¢¼ø±ðºÍ¼ì²échapter 2 description£¬identification and tests of drugs    ʵÑéÒ»  ÆÏÌÑÌǵÄÐÔ×´¡¢¼ø±ðºÍ¼ì²éÒ»    experiment 1 description£¬identification and tests of glucose    ʵÑé¶þ  ÒÒËáÇ⻯¿ÉµÄËÉ»òÒÒËáÇ⻯¿ÉµÄËÉƬµÄ¼ø±ðºÍ¼ì²é    experiment 2 description£¬identification and tests of hydrocortisone    acetate or hydrocortisone acetate tablets¡£    ʵÑéÈý  ¼×±½ßäßòµÄÐÔ×´¡¢¼ø±ðºÍ¼ì²é    experiment 3 description£¬identification and tests of mebendazole    ʵÑéËÄ  µäÐÍÖÐÒ©µÄ¼ø±ð    experiment 4 description£¬identification and test of typical tcmµÚÈýÕ  Ò©ÎïµÄº¬Á¿²â¶¨chapter 3 determination of drugs    ʵÑéÎå  ÁòËá¿üÄᶡ¼°ÆäƬ¼ÁµÄº¬Á¿²â¶¨    experiment 5  assay of quinidine sulfate and quinidine    s111flãÝtp tablpts      ʵÑéÁù  ÑÎËáÆÕ³¿¨Òò»ò×¢ÉäÓÃÑÎËáÆÕ³¿¨ÒòµÄº¬Á¿²â¶¨    experiment 6 assay of procaine hydrochloride or procaine    hydrochloride for injection    ʵÑéÆß  µâ±½õ¥¼°Æä×¢ÉäÒºµÄº¬Á¿²â¶¨    experiment 7 assay of iophendylate and iophendylate injection      ʵÑé°Ë  Í·æßÀ­¶¨¼°ÆäƬ¼ÁµÄº¬Á¿²â¶¨    experiment 8  assay of cefradine and cefradine tablets  µÚËÄÕ  Ò©ÎïÖÊÁ¿µÄÈ«¼ìÑé  chapter 4 drug analysis    ʵÑé¾Å  άÉúËØe»òάÉúËØeÈí½ºÄÒµÄÖÊÁ¿¼ì²é    experiment 9  analysis of vitamin e and vitamin e soft capsules      ʵÑéÊ®  °¢Ë¾Æ¥ÁÖÓ밢˾ƥÁÖ³¦ÈÜƬµÄÖÊÁ¿·ÖÎö    experiment 10 analysis of aspirin and aspirin enteric£®coated tablets    ʵÑéʮһ  ¸´·½»Ç°·¼×¶ñßòƬµÄÖÊÁ¿·ÖÎö      experiment 1 1  analysis of compound sulfamethoxazole tablets      ʵÑéÊ®¶þ  Í·æß¿ËÂå»òÍ·æß¿ËÂ彺ÄÒµÄÖÊÁ¿·ÖÎö    experiment 1 2  analysis of cefaclor or cefaclor capsules    ʵÑéÊ®Èý  ʯÝÅÆѵÄÖÊÁ¿¼ìÑé    experiment 1 3  analysis of acori talarinowii rhizoma    ʵÑéÊ®ËÄ  ÁùζµØ»ÆÍèµÄÖÊÁ¿¼ìÑé    experiment 14 analysis of liuwei dihuang wan     ʵÑéÊ®Îå  Ë«»ÆÁ¬¿Ú·þÒºµÄÖÊÁ¿¼ìÑé    expenment 15 analysis of shuanghuanglian koufuyeµÚÎåÕ  ÉúÎïÑù±¾ÖÐÒ©ÎïµÄ·ÖÎöchapter 5 q,mntitation of drugs in biological matrix     ʵÑéÊ®Áù  ÍÃѪÇåÖвè¼îµÄ¸ßЧҺÏàÉ«Æ×·¨²â¶¨    experiment 16 determination of theophylline in rabbit£¬s serum by hplc    ʵÑéÊ®Æß  °¢Ë¾Æ¥ÁÖ´úл²úÎïË®ÑîËáµÄѪ½¬Å¨¶È²â¶¨    experiment 17 determination of salicylic acid(sa)£¬metabolite    of aspirin(asa)in humans plasma by hplc    ʵÑéÊ®°Ë  ¸ßЧҺÏàÉ«Æ×·¨²â¶¨ÄòÒºÖб½°Í±ÈÍ×µÄŨ¶È    experiment 18 determination of phenobarbital in human£¬s urine by hplc    ʵÑéÊ®¾Å  lc¡ªms£¯ms·¨²â¶¨±È¸ñȮѪ½¬Öа¢ÆæùËصĺ¬Á¿    experiment 19 determination of azithromycin in beagle£¬s    plasma by lc¡ª¡ªms£¯msµÚÁùÕÂÉè¼ÆÀàʵÑé  chapter 6 designing experiment    ʵÑé¶þÊ®  À¼Ë÷À­ßòµÄ¼ø±ðʵÑé    experiment 20 identification of lansoprazole    ʵÑé¶þʮһ  À¼Ë÷À­ßòµÄÔÓÖʼì²éʵÑé    experiment 21  examination for impurities in lansoprazole        ʵÑé¶þÊ®¶þ  À¼Ë÷À­ßòµÄº¬Á¿²â¶¨ÊµÑé    experiment 22 content determination of lansoprazole     ʵÑé¶þÊ®Èý  ͪ¿µßòµÄѪҩŨ¶È²â¶¨    experiment 23 determination of ketoconazole concentration in plasma    ʵÑé¶þÊ®ËÄ  Ç忪Áé¿Ú·þÒºµÄÖÊÁ¿·ÖÎö    experiment 24 analysis of qingkailing koufuye   µÚÆßÕ  ·ÖÎö·½·¨ÑéÖ¤chapter 7  validation 0f analysis method      Ò»¡¢Ò©Æ·ÖÊÁ¿±ê×¼·ÖÎö·½·¨ÑéÖ¤Ö¸µ¼Ô­Ôò    ¶þ¡¢ÉúÎïÑùÆ··ÖÎö·½·¨µÄ»ù±¾ÒªÇó    1£®a guideline for the validation of analytical method adopted    in pharmaceutical      2£®the basic requirements for analytical methods of biological specimen¸½Â¼  ʵÑéÊÒ³£ÓÃÓ¢Óïappendix laboratory commonly used in english